185133. lajstromszámú szabadalom • Eljárás 1-hidroxi-okthidro-benzo-[c]kinolinok és származékaik előállítására

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185 133

IX. Táblázat

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[XXX általános képletíí vcg\ üleíek J

zw

r4

r6

ni/e (m+)

°C

D.p.

Tapasztalati

képlet

Számított C, H, N, %

Talált

C, H, N, %-0-CH(CH3 XCH2 )3 c6 h5

c2h5-H

405

155-6

c26h3103n

C = 77.00 H = 7.71 N = 3.45

C = 76.86 H = 7.62 N= 3.45

C = 78.05 N = 3.03

C = 78.16 N= 3.09

C = 77.81 N = 3.13

C = 77.73 N = 3.13

—0—CH(CH3 )(CH2 )3C6 h5

c4h9-H

433

160-2

c28h3503n

C = 77.56 H = 8.14 N = 3.23

C = 77.28 H = 7.92 N = 3.18

C - 77.56 N = 3.23

C = 77.86 N= 3.17

C = 79.80 N = 2.91

C = 79.64 N = 2.93

-0(CH2)3C6Hs

ch3-H

363

246-7

c23ii25o3n

C = 76.00 H= 6.93 N= 3.85

C = 76.19 H= 7.14 N= 3.89-C(CH3)2~C6Hs

ch3-H

355

261-2

c23n3302N

C = 77.70 H = 9.36 N = 3.94

C - 77.94 H = 9.21 N= 3.99-0(CH2>C6H5

ch3-II

349

248-250

c22h23o3n

C = 75.62 H = 6.63 N = 4.01

C = 75.26 H = 6.66 N = 3.93-OCH(CH3)(CH2)3C6Hs

H

H

377

170-173

c24h2-,o3n

C- 76.36 H = 7.21 N = 3.71

C = 76.38 H = 7.21 N = 3.85

C = 72.92 N = 4.25

C = 72.92 N= 4.42-0-CH(CH3XCH2)3C6Hs n-c3h7-H-164-166

c2,h3303n

C = 77.29 H = 7.93 N = 3.34

C = 76.97 H = 7.98 N = 3.41-0-CH(CH3)(CH2)3C6H5(a>

ch3-H

391

176-178

c25h29o3n

C = 76.69 H = 7.47 N = 3.58

C = 76.32 H = 7.36 N = 3.33-0-CH(CH3)(CH2)3C6H5(b)

ch3-H

391

172-174

C25 H2903N

C = 76.69 H = 7.47 N = 3.58

C = 76.40 H = 7.39 N = 3.51

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