189224. lajstromszámú szabadalom • Eljárás N,N-diacil-diamino-alkán származékok előállitására.
III. táblázat 189 224 2 O 4«tJ 1? Op. c# 0..i.gkdpl.i Anallxlt %. 'h-NHR /( ppa ) (adl.aOly) •zAftltûtt /»ért c 1 H 1 H T- â 1. ®-cv 112-114 C12H11N04 61.80 4.75 s.or 2.70 (»,4H.2CH2); 3.90 (233.24) 62.04 4.99 6.20 (•.2H.CH2); 7.30 (*.8H. ArCH.) CCOÇlj) 2. OfT us-lie C12H11N08 87.83 4.45 5.62 2.82 (*,4H.2CH2)i 5.60 (249.23) 87.64 4.82 8.88 (d.lH.CH); 6.70 (d.lH, OH), 7.30-7.60 C..5H. ArCH.) (OMSO-dg) H0-@-cv 3. 133-134 C12H11N06 87.83 4.48 6.62 2.80 C».4H.2CH2); 3.84 (249.23) 67.89 4.32 6.68 (..TH.CHj); 6.70-7.40 • («.BH.ArCH.) (COClj) 4. 99-100 C12M11N06 87.83 4.48 8.62 2.78 ( ,4H.2CH2)s 4.92 {^1 (249.23) 68.02 4.53 8.84 C»,2H.CH2), 6.80-7.50 '(■.SH.AîCH.) (COClj) 6. CH-*CH-CR.-flyV-0-CH_. 99-99 C16H17N08 60.19 5.37 4.39 2.80 (>.4H.2CH2)i 3.30 (319.33) 60.25 8.49 4.61 (d,2H.-CH2), 3.82 (*.3H, OCHj); 4.95 (*.2H.0CM2), 8.05-5.30 (a.2H,CH2), 8.80-6.35 («.ÎH.CH-); 6.50-7.00 (c.SH.ArCH. ) (COClj) «. CHj-CH-CH-^^- 0-CH2-142-144 C16H17N08 (319.33) 60.19 60.33 5.37 8.48 4.39 4.37 1.65 (4.3h .OH3), 2.U0. ((.4H.2CH2), 3.65 (t.3H. OCMj OCHj), 4.96 (4.2H.0CH2 ), 5.82-6.55 (..2H.CH.CH), 5.85 (.,3H,ArCH.) (COClj) ï. v-O-0-“*'ch2-ch»ch2 81-92 ^IT^S (303.33) 63.36 63.52 5.65 8.77 4.62 4.59 2.26 (• .3H.CHj), 2.60 (a. 4H.2CH2), 3.38 (d.2H.-CH2), 4.94 C..2H.0CH2), 5.02-5.33 (*.2H,CH2), 5.50-6.42 («. 1H.CH-), 6.50-7.02 (. .3H.ArCH-) (COClj) ». ^-3-CH2 97-98 C12H11H04S (268.30) 84.33 84.43 4.18 4.33 8.28 5.19 12.09 12.11 2.84 (« ,4H.2CH2), 3.94 (».2H,SCH2): 7.04-7.55 ( *. SH .ArCH. ) ( OMSO-dg ) a. O' 189-161 CoH^0^8 48.00 3.13 6.22 14.24 2.92 (« ,4H.2CH2), 7.20-(226.23) 47.81 2.93 6,08 14.11 7.52 (». 1H ,CH. ), 8.00-8.35 (■ .2H.2CH- ) (OMSO-dg) 10. O-cv 128-130 C10H9N048 (239.26) 60.21 80.33 3.79 4.00 S.65 5.79 13.40 13.22 2.80 (».4M.2CH2), 4.34 C».2H,CH2); 6.90-7.52 (•.3H.3CK-) (0«S0-d6) 10
