202820. lajstromszámú szabadalom • Hatóanyagként propénkarbonsav-származékokat tartalmazó fungicid készítmények és eljárás a hatóanyagok előállítására

21

HU 202 820 B

22

6,86-6,92 (2H, m), 7,0-7,16 (3H, m), 7,20-7,38 (5H, m), 7,47 (1H, s)

I. 399. 270 3,60 (3H, s), 3,76 (3H, s), 4,08 (2H, s),

6,80-7,58 (12H, m), 7,47 (1H, s)

V. táblázat folytatása

A tábla- A vegyü- Frekven- NMR spektrum vonalai, ppm

zat sorlet sorcia

száma száma MHz

I.

400.

400

3,59 (3H, s), 3,75 (3H, s), 4,18 (2H, s), 6,85 (2H, d), 7,00 (1H, s), 7,05 (1H, d), 7,10-7,35 (5H, m),

7,48 (1H, s), 8,10 (2H, d)

I.

401.

400

3,72 (3H, s), 3,88 (3H, s), 4,22 (2H, q), 6,83 (1H, s), 6,88-7,0 (3H, m), 7,21-7,42 (4H, m), 7,50 (3H, d), 7,60 (lH,s), 7,66 (lH,m)

I.

402.

400

3,70 (3H, s), 3,87 (3H, s), 4,70 (2H, s), 6,80 (1H, d), 6,95-7,05 (3H, m), 7,22-7,48 (5H, m), 7,59 (1H, s), 7,65 (2H,s), 7,92 (1H, d)

I.

405.

60

1,21 (9H, s), 3,42 (3H, s), 3,46 (3H, s), 4,80 (2H, s), 6,3-7,3 (12H, m), 7,31 (lH,s)

I.

406.

270

3,57 (3H, s), 3,71 (3H, s), 5,32 (2H, s), 6,92 (1H, d), 7,16 (2H, t), 7,24-7,43 (8H, m), 7,46 (1H, s),

7,66 (lH,d), 7,76 (lH,d)

I.

407.

270

3,51 (3H, s), 3,73 (3H, s), 4,59 (2H, d), 6,70 (1H, t), 6,96 (1H, d), 7,08 (1H, dd), 7,19 (1H, d),

7,22-7,37 (9H, m), 7,41 (1H, s), 7,48 (1H, d)

I.

408.

270

3,59 (3H, s), 3,71 (3H, s), 4,29 (2H, s), 6,94 (1H, d), 7,13-7,38 (10H, m), 7,45 (1H, s), 7,51 (1H, t),

7,63 (lH,d)

I.

409.

270

3,61 (3H, s), 3,78 (3H, s), 6,99 (1H, d), 7,15-7,36 (4H, m), 7,44 (1H, t), 7,50 (1H, s), 7,53-7,65 (2H, m), 7,78 (1H, t), 7,89 (1H, d), 8,10-8,19 (2H, m)

I.

410.

400

3,60 (3H, s), 3,75 (3H, s), 5,63 (2H, s), 6,6-7,3 (12H, m), 7,47 (1H, s)

I.

411.

400

3,60 (3H, s), 3,75 (3H, s), 4,8 (1H, d), 4,94 (1H, d), 6,6-7,7 (13H, m), 7,47 (1H, s)

I.

412.

270

1,67 (3H, d), 3,55 (3H, s), 3,70 (3H, s), 5,45 (1H, q), 6,5-8,1 (13H, m), 7,45 (1H, s)

I.

413.

270

3,59 (3H, s), 3,73 (3H, s), 5,17 (2H, s),

6,90-6,99 (2H, m), 7,12-7,43 (1H, m), 7,49 (1H, s), 8,08 (1H, s)

I.

414.

270

3,55 (3H, s), 3,70 (3H, s), 5,21 (2H, s),

6,91-7,0 (2H, m), 7,10-7,19 (1H, m),

7,21-7,38 (9H, m), 7,46 (1H, s), 7,53-7,60 (2H, m)

I.

415.

270

2,05 (2H, m), 2,78 (2H, t), 3,60 (3H, s), 3,75 (3H, s), 3,90 (2H, t), 6,5-7,3 (13H, m), 7,48 (1H, s)

I.

416.

270

1,78 (4H, m), 2,65 (2H, m), 3,60 (3H, s), 3,75 (3H, s), 3,9 (2H, m), 6,5-7,3 (13H, m), 7,47 (1H, s)

I.

417.

270

1,44-1,85 (6H, m), 2,62 (2H, t), 3,60 (3H, s), 3,75 (3H, s), 3,87 (2H, t), 6,48-7,31 (13H, m), 7,48 (1H, s)

I.

418.

270

3,61 (3H, s), 3,76 (3H,s),5,68

(1H, s), 6,8-7,6 (10H, m), 7,50 (1H, s), 7,8 (2H, m)

12