194541. lajstromszámú szabadalom • Hatóanyagként helyettesített maleinsavamid-származékokat tartalmazó fungicid készítmények és eljárás a hatóanyagok előállítására

1

194 541

2

A

példa X száma

X

R

R1

m R2

R3

n

R4

R5

R6

Y

Op. ( °C)

6

Cl

Cl

ch3

H

1 H

H

0

_

_

_

0

89-90

7

Cl

Cl

ch3

ch3

1 H

H

0

—

—

—

0

94-95

8

Cl

Cl

c6h5

H

0 -—

1

H

H

—

0

88-89

9

Cl

Cl

c6hs

H

1 H

H

0

—

—

—

0

132-133

10

Cl

Cl

ch2-c6h5

H

0 -—

1

H

H

—

0

123-124

11

Cl

Cl

ch3

H

1 H

H

0

—

—

2-C1

1

94-95

12

Cl

Cl

ch3

H

1 H

H

0

—

—

4-C1

1

109

13

Cl

Cl

ch3

ch3

1 H

H

0

—

_

4-C1

3

98-99

14

Cl

Cl

izo—C3H7

H

1 H

H

0

—

—

4-C1

1

91-92

15

Cl

Cl

ch3

H

1 H

H

0

—

...

2,4-Cl2

2

118-119

16

Cl

Cl

ch3

H

1 H

H

0

—

_

3,4-Cl2

2

74-79

17

Cl

Cl

ch3

ch3

1 H

H

0

—

—

3,4-Cl2

2

98-99

18

Cl

Cl

ch3

H

1 H

H

0

—

_

2,6-CIj

2

86

19

Cl

Cl

c6h5-ch2-H

1 H

H

0

—

—

2,6-Clí

2

108-109

20

Cl

Cl

ch3

H

0 -—

0

—

—

—

0

62-65

21

Cl

Cl

ch3

H

0 -—

0

—

—

4-CH3

1

79-80

22

Cl

Cl

ch3

H

0 -—

0

—

—

terc-C4 H9

1

olaj JR: 1740, 1360, 880 cm'1

23

Cl

Cl

ch3

H

1 H

H

1

H

H

—

0

88-89

24

Cl

Cl

n—C3H7

H

0 --0

—

—

—

0

olaj JR: 1740,1350, 1070 cm'1

25

Cl

Cl

ch3

H

1 H

H

1

H

H

2-C1

1

98-100

26

Cl

Cl

ch3

H

0 -—

0

—

—

4-C1

1

101-102

27

Cl

Cl

ch3

H

0 --0

—

—

4-OCH3

1

olaj JR: 1740, 1510, 1250 cm'1

28

Cl

Cl

ch3

H

0 --0-—

3-CF3

1

olaj JR: 1740, 1350 cm'1

29

Cl

Cl

ch3

H

1 H

H

1

H

H

4-C1

1

68-71

30

Cl

Cl

ch3

H

1 H

H

1

H

H

2,4-Clj

2

85

31

Cl

Cl

ch3

H

1 H

H

1

H

H

3,4-C i2

2

66-68

32

Cl

Cl

ch3

H

1 H

H

1

H

H

2'6-Cl2

2

82-83

33

Cl

Cl

ch3

H

1 H

H

1

H

H

4-CH3

1

99-101

34

Cl

Cl

ch3

H

1 H

H

1

H

H

4-0CH3

1

106-107

35

Cl

Cl

ch3

H

1 H

H

1

H

H

4-terc-C4H9

1

64-65

36

Cl

Cl

ch3

H

0 -—

2

H

H

—

0

olaj JR: 1735, 1360 cm'1

37

Cl

Cl

ízo-C4H9

H

0 -— .

2

H

H

—

0

olaj JR: 1735, 1365,880 cm'1

38

Cl

Cl

ch3

H

0 -—

2

H

H

2-Cl

1

olaj JR: 1735, 1360 cm'1

39

Cl

Cl

izo—C4H9

H

0 -—

2

H

H

2-Cl

1

olaj JR: 1735, 1360, 880 cm'1

40

Cl

Cl

ch3

H

0 -—

2

H

H

4-Cl

1

olaj JR: 1735, 1360, 1090 cm'1

41

Cl

Cl

íso-C4H9

H

0 -—

2

H

H

4-Cl

1

olaj JR: 1735, 1365, 1095 cm'1

42

Cl

Cl

ch3

H

0 -—

2

H

H

4-CH3

1

olaj JR: 1735, 1370, 880 cin'1

43

Cl

Cl

ch3

H

0 -—

2

H

H

3,4-Cl2

2

olaj JR: 1735, 1365 cm'1

44

Cl

Cl

ch3

H

0 -— .

2

H

H

4-OCH3

1

olaj JR: 1740, 1250,1040 cm'1

45

Cl

Cl

ch3

H

2 H

H

0

—

—

—

0

olaj JR: 1735, 1365 cm'1

46

Cl

Cl

ch3

H

2 H

H

0

—

—

2-Cl

1

olaj JR: 1735, 1390 cm'1

47

Cl

Cl

ch3

H

2 H

H

0

—

—

4-Cl

1

olaj JR: 1735, 1385 cm'1

48

Cl

Cl

ch3

H

2 H

H

0

—

—

3,4-Clj

2

olaj JR: 1740, 1390 cm'1

49

Cl

Cl

ch3

H

2 H

H

0

—

—

4-CH3

1

olaj JR: 1740, 1380 cm'1

50

Cl

Cl

ch3

H

2 H

H

0

—

—

4-OCH3

1

olaj JR: 1735, 1400 cm'1

51

Cl

Cl

c2h5 ;

H

2 H

H

0

—

—

—

0

olaj JR: 1735, 1390, 700 cm'1

52

Cl

Cl

ch3

H

1 ch3

H

1

H

H

—

0

olaj JR: 1735, 1390, 880 cm'1

53

Cl

Cl

ch3

H

1 ch3

H

1

H

H

3-C1

1

olaj JR: 1735, 1360, 880 cm'1

54

Cl

Cl

ch3

H

0 -—

2

H

Hu.

—

0

106-109

ch3

ch3

5